Questions tagged [equipment]
Questions regarding the equipment used in labs (such as flasks, tubes etc.), their operation and maintenance.
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Is it critical to match vacuum pump oil to specific pump?
We have rotary vane vacuum pumps of many makes, models, and ages, but superficially they seem remarkably similar. Each has a recommended pump oil (that is, if we can find the documentation); often ...
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Why does glass etching cream contain sulfuric acid?
The MSDS for various glass etching creams all show that they're primarily composed of 4 substances (the composition percentages vary):
Ammonium Bifluoride - 20 - 40%
Sodium Bifluoride - 5 - 10%
...
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What's the purpose of this vintage glassware?
I found this glassware in a phytochemistry lab abandoned in the 1990ies. The piece itself was shelved in the storage room, thus probably already obsolete back then.
The device, entirely glass, is a ...
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Using a vintage lab balance scale with a chain-dial
I have obtained an an antique Philip Harris balance scale in good, but condition aside from a lot of corrosion on the brass. I can't find a model number on it and am not sure of it's actual age, but I ...
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What is the sample density used for a buoyancy mass correction?
For a lab exercise to calibrate volumetric glassware I was given the follow equation to correct weighings for the density of air:
$$m_\mathrm{c} = m_\mathrm{s}\,\frac{1 - \rho_\mathrm{a}/\rho_\mathrm{...
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Can I use a mechanical pipette to transfer strong acid?
I am an undergraduate student majoring in physics. I am looking for the best method to accurately measure the volume of strong acids like hydrobromic $(w(\ce{HBr(aq)}) = 48\,\%)$ and hydroiodic $(w(\...
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Can the stability of organic / inorganic salts be negatively impacted under the freezing point of water?
Appart from biological stuff that can be damaged by the formation of crystals, is there any mechanism that could cause or accelerate the degradation of organic or inorganic salts when stored below the ...
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Is Silica Gel fit for Ultra-High Dessication?
I had the (perhaps wrong) notion that silica gel wasn't that strong of a dessicant, especially compared to CaO, MgO, CaSO4, H2SO4, KOH, Mg(ClO4)2), but I've been exposed to information* that might ...
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Can Choline Chloride be Dehydrated with Calcium Sulfate?
Standard procedure to bring choline chloride to dryness is to store it in a vacuum desiccator over P2O5 or Mg(ClO4)2.
I however have access to neither of those compounds.
Can I instead dehydrate ...
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Would a 0.3 micron filter be effective in blocking formaldehyde fumes produced by curing cyanoacrylate?
I’m looking into purchasing a mask that blocks particles larger than or equal to 0.3 μm in size. I’m hoping it blocks the formaldehyde fumes produced by curing cyanoacrylate.
How effective such mask ...
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Why do Büchner funnels have no glaze on the top rim?
I have a question about Büchner funnels (just out of pure curiosity). The funnels I have seen have no glaze on the top rim. Actually, the question is why the top end is not glazed. Does it have any ...
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Which vessel materials are compatable with magnetic stirrers?
I am shopping for some metal pans and beakers for use on my magnetic stirring hotplate. I do not want to block the magnetic coupling of the stir bar. The question is which common alloys are compatible?...
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Connect glass tubes to a graham condenser
I am currently making a syphon coffee maker such as this one:
However, I find that all the silicon tubing used on this image between the condenser and the boiling flask / between the condenser and ...
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Experimental setup
I would like to know your opinion regarding the setup of a system for oxygen purging with nitrogen. Before ordering the necessary materials, I'd like to be sure if this setup is feasible or if it can ...
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How should you report measurements and uncertainty for a measuring cylinder with 0.5 mL graduations?
I understand that a common convention is to report the uncertainty of an analogue instrument as plus or minus half of the smallest scale division.
By this logic, a measuring cylinder with $\pu{0.5 mL}$...
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What material should my evaporation dishes be made of to combat static charge buildup?
I have great difficulties moving very fine powders from a drying dish (glass) into small plastic containers using a metallic spatula due static charging. I have to scratch a lot inside the glass ...
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Best bet for separating fused glassware
I have a sintered glass funnel stuck in a flask with a 24/40 ground glass joint.
I regularly used this glassware to process very dilute solutions of uncured photopolymer resin dissolved in ethanol. ...
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Which is a more accurate scale for a chemistry high school lab - a triple beam balance or a digital balance and why?
I would like to ask the experts of this chemistry community their opinions on which balance is more accurate and effective to use in a high school chemistry lab- a triple beam balance or a digital ...
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Is there a simple way to distinguish grades of purity for copper metal?
Is there a simple way to distinguish different grades of fine copper purity (on a trace metal basis) that can be carried out in a small lab?
Specifically, I would like to be able to differentiate 4N, ...
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Can stainless steel be electrically insulated with (oven-dried) Sodium Silicate Solution?
Can I electrically insulate stainless steel by painting Sodium Silicate solution on it and heating it to 200C for 30min or so?
The solution should be conductive, and I've been told (to be verified) ...
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Will Sodium Polyacrylate (SAP) absorb the gas from liquid ammonia?
I'm considering using sodium polyacrylate grains to absorb spills of a relatively strong Ammonium Hydroxide solution. Will the SAP (super absorbent polymer) only absorb the water, and in effect make ...
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Microfiltration for saturated solutions of highly hygroscopic compounds?
Is it possible to pass saturated solutions of compounds with very high solubility through filters with small pores (e.g. passing a saturated aqueous ZnCl2 solution at 90C through a 2mcm glassfiber ...
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Does adding NH3 to an HCl solution facilitate the dissolution of aluminum compounds?
If we compare the two solutions hereafter, which one would better leach/dissolve aluminum metal/compounds present at/near the inner surface of the glass:
Solution A: $10\,\%\, \ce{HCl + H2O}$
Solution ...
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Appropriate ways to remove aluminum from the surface of glass?
I'm looking for a way to treat the surface of borosilicate glassware such that it won't contaminate solutions of puriss reagents in conditions that pure $\ce{SiO2}$ wouldn't, yet keep the bulk ...
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Trial by fire: Safely heating sand without it agglomerating?
Wikipidia quotes a melting point of 1713C for sand.
I went on the beach to get some sand. I assume it's a mix of all kinds of stuff.
The finality is to prepare a big pile of clean sand to use as ...
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How does functionalized activated charcoal work?
If I understand correctly it is possible to trap stuff inside activated charcoal (AC) pores to give it specific retention properties (by exposing it to functionalizing compounds while heated to open ...
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Can I engrave borosilicate glassware without compromising its structural integrity?
Can I use a pen engraver (the kind that's like a tattoo gun with a diamond tip) to engrave my initials on labware without compromising it? I am in a lab space with a shared acid wash, and my glassware ...
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Is it better to use a smaller, more accurate measuring cylinder several times or a larger, less accurate one for the same volume?
I need to measure out 70 ml of liquid.
I have a 10 ml measuring cylinder with a maximum uncertainty of 0.1 ml and a 100 ml measuring cylinder with a maximum uncertainty of 1 ml.
I've calculated that ...
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How to identify a blow-out pipette?
Is my pipette a blow-out pipette?
I suspect that it is a blow-out pipette, though the double lines aren't rings. My guess is it is a TC blow-out pipette. It's a big 50 mL pipette, longer than my arm.
...
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What is the purpose of this glassware?
I have seen these small test tube looking doohickeys being supplied from many chinese suppliers, but never with any description as to what they are for. They almost invariably have the description &...
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Does mercury react with polycarbonate?
Looking around at various material compatibility charts, they seem quite divided on the compatibility of metallic mercury and polycarbonate. Some sources (here, here, or here) indicate that ...
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What is the product of ammonia reacting with silicone?
I used a soft silicone hose to carry ammonia at ~70 °C. I was surprised to later find the hose had hardened.
A quick materials compatibility search for silicone had given me a lot of info but an "...
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HDPE vs PP for storing pure aldehydes
I know both HDPE and PP have at least some degree of resistance to aldehydes, esters and aliphatic hydrocarbons.
I am concerned however about minute contamination over time of pure samples and so I ...
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Any plastic for long term storage of Puriss. Ethanol?
I'm being offered to share some puriss Ethanol. Can I store it long term in any plastic container without the slightest contamination/reaction from the plastic? I have HDPE, PET, but I could buy ...
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Safest way to conduct a reaction with bromine under reflux conditions
I am conducting an electrophilic aromatic bromination reaction according to literature. The substrate and intended substitution pattern do not matter, but the reported procedure requires the dropwise ...
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Reduction by Activated Carbon
Does reduction by carbon itself occur when filtration is performed using activated carbon? Is it part of the central mechanisms involved in activated carbon filtration?
One of the specificities of all ...
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Experience with PTFE tubing & glass connectors?
I'm wondering which PTFE tubing size to get to connect to normal 10mm OD glass connectors. For a silicon hose I would take an ID of 8-9mm as it is flexible but I think PTFE is quite rigid.
Anyone has ...
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What has happened with the pH-meter?
The glass sensor has became red inside like something melted. I stored it in a liquid with pH that mentioned in the manual. What is that and why could that happen, how often that happens with pH-...
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Sintered vs perforated plate Büchner funnels
I just bought a sintered-glass style Büchner funnel for some vacuum filtration tasks. There's two issues I'm having with it:
Filter material, especially activated charcoal, ends up stuck in the glass ...
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when using glass to glass stoppers, is it best to have them dry or use lubricant?
I have some glass flasks that have glass stoppers. It’s basically the typical glass stopper with the frosted tip which fits into a glass opening. Basically think of a typical glass volumetric flask. i ...
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Affordable, non-contaminating flexible tubing for common acids
Which tubing material is affordable, flexible, widely available, and suited for transporting very pure acids ("puriss." products) in their most concentrated form without contaminating them?
...
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What kind of filter can remove zeolite dust from ethanol?
I only really have high school level knowledge of chemistry, and also I don't really own any lab equipment.
I'm using 3A zeolite molecular sieves to dry ethanol (and sometimes isopropanol) and they ...
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Is the width of a Soxhlet Condenser Inherent to its Function?
Soxhlet extractors are often coupled to a specifically designed condenser with a very large lower joint.
Is this inherent to it's function as a condenser in the apparatus or only because the Soxhlet ...
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Confused Reading of Pressure on Vacuum Gauge [closed]
I have a gauge used to measure vacuum but I'm a bit confused as the measurements state "Hg" (I would have supposed inches of mercury except it goes to -30) and "Bar" going to minus ...
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What the difference in data if calibrate pH-meter with 2 and 3 solutions? [closed]
pH-meter (12 bucks one) can be calibrated with 2 different solutions (let's say 4.0 and 6.86), but as an option 3 can be used (4.0, 6.86 and 9.18). If I use 2 instead of 3, what error I'm going to get....
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Which Additives May be Present in Cellulose Filter Paper? [closed]
I'm wondering what, other than cellulose, might be contained in filter paper (the kind routinely used in Buchner filters / normal funnels).
A search here on Chemistry Stackexchange shows that at least ...
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Compact way to regulate 3000psi (200bar) down to 30psi (2bar)?
This was originally posted on the Lego page, and closed because it's not actually about Lego itself. I thought I'd give them a chance first, in case someone had done this already and had some ...
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Looking for advice regarding a larger scale soxhlet extraction
I have successfully completed a few soxhlet extractions at a much smaller scale using a soxhlet extractor with ~200ml capacity. With that, I was able to extract from ~100g of pre-powdered, sonicated ...
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can i use an isobutane stove (like jetboil) or butane blowtorch with borosilicate glass?
I don't have a bunsen burner, but have a camping stove (similar to https://www.amazon.com/Stansport-183-B-Isobutane-Backpack-Stove/dp/B004EPWM5S) and a blow torch. I'd like to do some distillation ...
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cheap anti-fog agent!
What are some safe and widely available alternatives to specifically formulated anti-fog sprays/treatments? Specifically for use on glasses, goggles, and face shields.
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