Questions tagged [separation-techniques]
For questions about the separation of mixtures and solutions into pure compounds
26
questions
3
votes
1answer
28 views
HPLC Columns For Compounds Not Soluble In Non- Or Low Polar Solvents [closed]
Can someone recommend HPLC columns for compounds which are not soluble in no- or low polar solvents (hexane, isopropanol, toluene, and dichloromethane)?
0
votes
0answers
23 views
coffee concentrate and water separated after 2 hours. How/why?
I'm asking because this makes no sense to me and making sure I'm not stupid.
I brewed 10 gallons of cold brew concentrate(TDS 12.2) and mixed it with 10 gallons of water.
I moved 10 gallons of the ...
3
votes
1answer
133 views
How to conveniently separate Cd impurities from ZnO without contaminating it?
How could I separate Cd impurities from ZnO without contaminating it and without using overly expensive equipment or extremely dangerous solvents?
I don't want to contaminate it by introducing other ...
1
vote
0answers
30 views
Protein purification pressure limits confusion, about the X-MPa limit for FPLC?
I have always been a bit confused about column pressure limits. I have to elaborate a bit on the problem to get to my question:
In protein purification we use the äkta purification machines (e.g. ...
3
votes
1answer
257 views
How to remove sugar from juice
My son has autism and we noticed that blueberries make him feel much better. The problem is blueberries contain sugars which interfere with diet he has (low carbohydrate).
How do I filter out the ...
1
vote
2answers
59 views
How do you get contents of large flask into a smaller separatory funnel?
Separatory flasks that I use have a ground glass joint, but it is not clear how that joint is to be used. Videos I have seen just show people pouring stuff into the throat of the funnel.
Normally the ...
2
votes
0answers
48 views
Is there a way to form only ortho product without using fractional distillation?
Using benzene and ethane as your only source of carbon in the final molecule, synthesize the following using any useful reagents. Reaction must form pure ortho compound.
I have to form the ...
2
votes
0answers
99 views
What is the principle of “scrubbing” in liquid extraction or solvent extraction?
There are many steps in solvent extraction:
Extraction
Scrubbing
Back extraction
I understand the 1st and the 3rd.
What is the principle of scrubbing?
Is it just washing the organic phase?
How ...
2
votes
1answer
272 views
Shea Stearin Extraction by Dry Fractionation
I have been able fractionate palm oil and extract palm stearin using the following method:
Melt the palm oil (over 80 °C)
Keep the melted oil at 33.5 °C for 24 hours (using an immersion circulated ...
-1
votes
1answer
79 views
Reasoning about a separation problem [closed]
Describe exactly how you would go about separating a mixture of the three water-insoluble liquids, aniline (b.p. 184 °C), n-butylbenzene (b.p. 183 °C) and n-valeric acid (b.p. 187 °C), recovering each ...
-1
votes
1answer
549 views
Reaction between HCl and NaHCO3 [duplicate]
I want to know why in the reaction between HCl and NaHCO3, we have CO2 and H2O instead of H2CO3 ?
4
votes
1answer
115 views
Recover Solder (Sn-Pb) from wires
I have began to do an "art project" which utilizes solder as main material.
While I know that solder is cheap and easily found in multiple shops, I have set my mind on using recycled solder from out ...
1
vote
2answers
270 views
How to separate two liquids with both having the same properties?
I was curious if it was possible to separate such liquids e.g. two vegetable oils that happened to have different ingredients, so it is a different liquid, but the same density etc.
-1
votes
1answer
55 views
Separating 2 chemicals [closed]
Is it possible to separate two chemicals with slightly different melting points? Can this be done with the use of a lab freezer? As MP is -44 and The other is -61 - -59 °C.
Will it solidify these ...
2
votes
1answer
102 views
Separating specific components of a PUREX raffinate
The PUREX extraction in nuclear fuel reprocessing leaves behind a nitric acid raffinate full of (mainly) 'fission products', which are a diverse set of elements produced by fission in a nuclear ...
3
votes
1answer
59 views
Is the pressure in an HPLC system the same throughout?
I'm not sure if I'm articulating myself well enough, but here's my problem: I have a current HPLC system, where we typically have backpressure readouts of around 15 MPa. We are looking to get a new ...
1
vote
0answers
33 views
Hypothetically, can sufficiently powerful centrifugation separate normally miscible chemicals of differing densities?
Centrifugation is used to separate phases in suspensions by density. I read that this is not possible with colloids and solutions, but the distinction between the three seems to be optical properties ...
0
votes
3answers
393 views
Why does a molecular sieve work for gas separation?
I was looking at membrane separation of air to nitrogen / oxygen and saw some details on the molecular sieve which on Wikipedia states you can get much higher purity from an adsorber / sieve, but when ...
-1
votes
1answer
2k views
How would you separate sodium chloride and copper sulfate?
I've tried dissolving both compounds in water and evaporating the mixture, but this leaves a combination of brown and green crystals. Is there was any way to cleanly separate both compounds? Any ...
1
vote
0answers
42 views
Removing chloride ions from humic acid purification
I used HF and HCl in humic acid purification, and now I need to remove the Cl ions from solution. What should I do to remove the Cl ions? Do I just wash it with distilled water, or is there another ...
2
votes
1answer
2k views
How to separate sodium carbonate from sodium hydroxide?
I got a drain cleaner in dust form, which consists of $\ce{Na2CO3}$ and $\ce{NaOH}$. I wanted to extract the $\ce{NaOH}$ so I tried to heat the mixture in order to just melt the sodium hydroxide, but ...
3
votes
1answer
83 views
etymology of supernatant
Why do we call a solution that has been centrifuged a supernatant? It seems to me that a "natant" should be something that floats (from Latin "natare" meaning "to swim"), and a "supernatant" should be ...
3
votes
1answer
65 views
Using cryptands to make a negatively-charged solution?
In our discussion group, my friend mentioned that metal cations can be separated from other cations in solution using cryptands. After addition of the cryptands to the solution of the cations, ...
1
vote
2answers
406 views
How can I separate these two alcohols from each other out of the aqueous solution?
I have the following question for homework and am stumped. I am tasked with separating 3-(2-methoxyphenoxy)propane-1,2-diol and (1R,2S)-2-(methylamino)-1-phenylpropan-1-ol. They are both solvated in ...
2
votes
1answer
1k views
Separating glucose and fructose
If I have a mixture of glucose and fructose in aqueous solution, what is the simplest method to separate them? Heating to 110 °C to melt only the fructose would probably work theoretically, but this ...
11
votes
5answers
20k views
Is it possible to separate/remove sugar from common drinks, such as juice?
Is it possible to remove sugar from a drink (for example, juice) using common household equipment?
