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Some experimental data after a 4 liter jug of 5% distilled white vinegar accidentally froze at -25°C: The first 0.5 liter to melt out had an acetic acid concentration of about 13%, substantially above the starting concentration, and a pungent vinegar smell. The next 1 liter to melt out had an acetic acid concentration of about 7%. The remaining ice was very ...


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