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Use this tag for questions relating to organic molecules and their properties (structure of organic molecules, spectroscopic properties, reaction mechanisms, stereochemistry etc). DO NOT use this tag as the only tag in your question, as this tag by itself cannot appropriately classify your question. Always use this tag in addition to other more specific tags.
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Which process would separate the mixture of toluene, cyclohexane and water?
Need to check ternary phase diagram of cyclohexane:toluene:water.
There are azeotropes water:toluene at 89 °C (0.49:0.51) and water:cyclohexane at 69 °C (30:70).
Hence, first separate water if you can …