Questions tagged [x-ray-diffraction]

X-ray diffraction is a method to obtain the crystal structure of a compound. This tag is also appropriate for x-ray powder diffraction.

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What is “detwinning” as a 2D crystallography technique?

The Phys.org article Iron selenide revealed as 'garden-variety iron-based superconductor' is quoted below. Normally I would hesitate to quote so much but in this case it all seems germane. Question: ...
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X-ray structure analysis mirrored coordinates?

How to ensure, that X-ray crystallography structure analysis was done right to provide correct, non-mirrored atomic coordinates? Example: Following Wikipedia image, is generated from data taken from ...
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Why are certain reflections forbidden in body centered cubic and face centered cubic structures?

I know that for body centered cubic structures the allowed reflections only happen if h+k+l is even and reflections are forbidden is h+k+l is odd, and for basic face centered cubic structures (...
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XRD-Amorphous materials

I am interested in sealing some air-sensitive samples inside of xrd-amorphous material to allow for XRD and hopefully XRD-texturing analysis. Of course, Kapton is the common material used for this ...
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What is the crystal structure for a crystal where the ratio of the squares of the angle peaks is 0.825?

I followed this and it gives an example of how to identify a crystal structure using XRD data. I have an unknown alkali halide where two peaks were found at $2\theta =25.66$ and $2\theta = 28.3$. I ...
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In powder x rd, if the crystals are randomly oriented ,why then do we get Debye rings and not random patterns?

In powder x-ray diffraction ,as I have learnt the sample is multi-crystalline.So if x-ray is diffracted through these randomly oriented crystal grains, aren't we supposed to get a random pattern?
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What can be concluded from two different values for the interplanar distance between planes of atoms in an X-Ray diffraction experiment?

I analyzed an unknown Alkali Halide crystal using x-rays from a copper source. I need to find the d-spacing for this crystal, i.e. the interplanar distance between planes of atoms. I found my $K_\...
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Image formation in LEEM

currently I'm studying for my master's examination in physical chemistry. The topic will be surfaces and catalysis. To prepare myself I'm reading "Surface Science - An introduction" by Oura. ...
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Obtaining atomic form factor from electron density?

I know that atomic form factors for x-ray scattering are obtained by Fourier transform of the electronic charge density. I am looking for a citable elementary source (book, review, article) which ...