Questions tagged [precipitation]

For questions related to the chemical reactions and processes that result in a chemical reaching its solid phase.

32 questions with no upvoted or accepted answers
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279 views

DIY hand sanitiser solution forms spongy substance

I am trying to make my own hand sanitiser since it’s sold out everywhere. The formula I use is 1 part aloe vera gel in 2 parts 100% isopropyl alcohol. The problem is when mixing the two, the solution ...
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270 views

The behaviour of Ag3PO4 in solution

To a $\pu{1L}$ flask, we add $\pu{4.1900 g}$ ($\pu{0.01001 mol}$) of $\ce{Ag3PO4}$, then fill it up with water. Knowing the following constants, we are asked to find the concentration of all species ...
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162 views

How to prevent Tin ions from precipitating as Tin(II,IV) Hydroxides

Alright, so Tin ions in most of it's salts have the propensity to form Tin(II,IV) Hydroxides and then precipitating out of aqueous solutions. What can I throw in the solutions to prevent this? Using ...
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123 views

How much of the anion species is left over after the first precipitation?

Some barium chloride is added to a solution that contains both $\ce{K2SO4}$ ($\pu{0.050 M}$) and $\ce{Na3PO4}$ ($\pu{0.020 M}$). (a) Which begins to precipitate first: the barium sulfate or the ...
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106 views

Can I extract solid sugar from any fruit juice at home?

The goal here is to isolate the sugar from all other compounds in the juice. In this case, I'm using apple juice and grape juice. The sugar does not need to be edible, as it is being used to make r-...
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48 views

Which salts precipitate from a potassium/sodium chloride/sulfate solution?

This is not a homework question. I am not in any course of study. The following question arises from my personal curiosity. If 1 mole of sodium sulfate and 2 moles of potassium chloride are dissolved ...
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25 views

Cleaning a stubborn Electrospray residue

I have an electrospray ionization capillary tip that sprays into a chamber that contains some circuit boards. An aqueous CsI sample is apparently causing a white residue to build up on these boards ...
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76 views

Generating Precipitation Diagrams with CompuTherm Pandat

I am trying to develop precipitation diagrams for an Ag-Cu-Sn alloy to figure out the kinetics involved using the CompuTherm Pandat Software (Demo Version). The precipitation diagrams need the ...
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42 views

Why does the reaction between copper(II) ion and iodide ion proceed even though the E_cell of the set up is negative?

(iii) Another example of a reaction that does not agree with the theoretical prediction is the reaction between $\mathrm{Cu}^{2+}$ and $\mathrm{I}^{-}$ according to the equation below. $$ 2 \mathrm{Cu}...
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60 views

How do I get calcium citrate to precipitate in experiment on extraction of citric acid from juice?

I was planning to extract citric acid from mango juice by first using Aspergillus niger fungus by fermentation to convert the mango juice to citric acid, then extracting by first adding sodium ...
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55 views

Why is hydrated barium peroxide used in the preparation of hydrogen peroxide?

I read about the laboratory method of producing hydrogen peroxide. The chemical reaction in question is: $$\text{BaO}_2.8\text{H}_2\text{O} + \text{H}_2\text{SO}_4 \rightarrow \text{BaSO}_4+\text{H}_2\...
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89 views

Reaction of Glucose + NaOH + PVP

I'm trying to synthesize of silver particles by using glucose as reducing agent, PVP as dispersant, and NaOH as pH control. Before adding silver nitrate solution, I've produced a solution which is ...
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41 views

how can I predict the rate of water ions precipitation on a surface?

Consider a titanium pot that contains 1kg water with the following ions: $[Ca^{2+}]=22000$ ppm, $[Mg^{2+}]=1500$ ppm,$[Sr^{2+}]=791$ ppm,$[Na^{1+}]=48000$ ppm,$[Cl^{1-}]=120000$ ppm,$[SO_4^{2-}]=...
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288 views

Fast and complete ways to remove chloride from solution (sub ppb levels)

Main question: We are trying to reduce the chloride concentration in a solution to sub-ppb levels. I have to dissect a fruit fly in this solution so I am interested in removing any chloride that is ...
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68 views

Triiodide ion gravimetric analysis Reaction Equation

Last week I did a gravimetric analysis from the following reaction. $\ce{AgNO3 + (CH3)4N+I3- -> AgI(s) + (CH3)4N+NO3- + I2}$ The objective was to identify if my reactant was triiodide or ...
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82 views

What chemicals could be added to human urine to cause harmful chemicals to precipite out?

What chemicals could be added to human urine to render it drinkable with no harmful side effects? Urine is salty and contains other dissolved solids. Thus, drinking untreated urine would result in ...
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53 views

Precipitation occurred when adding vanilla extract to oak extract. What caused this?

Sorry if this is a very obscure question, but I don't know where to ask it. 120ml of oak extract, made by soaking oak chips in ethanol, was added to a flask. At this point, the solution was very dark ...
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379 views

Precipitation of Calcium ions in basic Sodium Hydroxide solution?

I recently conducted an EDTA titration of milk to find its Calcium contents. I got a value significantly smaller than the theoretical value. (≈10 times smaller). I made $50ml$ samples to which I added ...
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89 views

Stoichiometry reactions for water clarification

If ferric chloride was added to a water sample which had calcium bicarbonate alkalinity present, would the reaction be a ‘stoichiometry reaction’ or a ‘limiting reagent reaction’? For example, if 1 g ...
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17 views

Can two two-material composite precipitation methods be used to make one three-material composite?

There are many methods used in the synthesis of cellulose nanocomposites, including Fe₃O₄@Cellulose in urea, ammonia, and water solution and immersing the product in sulfuric acid, or somewhat ...
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33 views

Identification of salts observed in steam vaporiser

Recently I observed some precipitated salts in steam vaporizer after completion of vaporization. I am guessing that some of the white particles may be calcium carbonate ($\ce {CaCO3}$) formed from ...
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34 views

Adding aluminum sulfate to neutralize an aqueous solution of sodium silicate with pH of 12.6

How much aluminum sulfate do I need to add to an aqueous solution of sodium silicate to neutralize the solution (pH from 12.6 to 7)? For a water treatment school project, we remove sodium silicate ...
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21 views

Preventing Precipitation/Undilution: Shall I Try Another Solvent?

Thank you for your time in advance. Our facility is about $\pu{4000 ft}$ in terms of elevation. One of the main chemicals we manufacture is RAD140 or $\ce{C20H16ClN5O2}$. We use DMSO ($\ce{(CH3)2SO}$),...
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28 views

Solubility Product, and it's relation to solubility

In order to remove temporary hardness of water, it is boiled. On boiling, while Ca(HCO3)2 gives CaCo3(ppt.) , Mg(HCO3)2 gives Mg(OH)2(ppt.). According to my book precipitation of Mg(OH)2 occurs due to ...
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10 views

Material properties differing between vacuum or pressure filtration

During vacuum filtration of a very fine suspension, all solids that need to be removed are, but there is minimal solids loss. If the same material is pressure filtered (1-2 bar), desired solids ...
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29 views

Ideal characterization technique to study behavior of heated metal nitrates

I have 3-4 metal nitrates as precursors for my coprecipitation reaction. I need to study the behavior of each individual nitrate and also of various combinations at 60 degrees Celsius, which is my ...
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20 views

Method to find out the amount of solvent replaced by another solvent

So I am performing a relatively simple coprecipitation experiment to synthesize ceramics. All my precursors are in aqueous solutions. But due to the high surface tension of water, drying the water is ...
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28 views

Can classification techniques used for identifying solids be used to identify precipitates?

I am preparing for an assessed practical experiment where an unknown precipitate must be identified. I know that precipitates are insoluble, and my textbook says they are considered to be solid with ...
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1k views

Eutectic Phase Diagram of Al-Si Analysis

Hello, How can I know from this phase diagram: 1. The composition of the alloy Al-Si that allows precipitation to occure? 2. The range of temperatures where the Al-Si is soluble? 3. The range of ...
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1answer
51 views

How to distinguish between iron and nickel based on the mass of precipitate formed with sodium hydroxide?

For the reactions shown below, we added $\pu{5.00 mL}$ of $\pu{0.0390 M}$ $\ce{NaOH}$ to a test tube containing one of the two cations $\ce{Ni^2+}$ or $\ce{Fe^3+}$ and recovered $\pu{0.00695 g}$ of ...
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1answer
116 views

Determine concentration of phosphate after copper(II) oxalate is precipitated

Solution with $\ce{Na3PO4}$ with $\pu{0.02 M}$ concentration and $\ce{Na2C2O4}$ with $\pu{0.03 M}$ concentration. I add excess $\ce{Cu(NO3)2}$ very carefully – tiny amounts. What will be my $\ce{PO4^...
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1answer
37 views

Selectivity of metal nitrates towards ammonium bicarbonate

I am performing coprecipitation reaction, and in the precipitating step, I have a bunch of metal nitrates(ferric nitrate, aluminium nitrate and barium nitrate)in a solution reacting with ammonium ...