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4 votes
1 answer
69 views

Refrigeration for Cryochemistry −35 °C

I need to cool a tube containing liquid to −35 °C for a cold chemical experiment that will last about a week. The glass vessel I need cooled is 500 mL in volume and will be giving off $\ce{H2S}$ gas. ...
Dale's user avatar
  • 2,682
2 votes
1 answer
2k views

Where can I find CAD blocks for lab glassware?

I want to draw a sketch of my apparatus for my report. I am conversant with the AutoCAD drafting software. Where can I download CAD blocks for commonly used labware items (like round bottom flask, ...
Abhishek's user avatar
  • 121
3 votes
1 answer
162 views

Sodium by electrolysis through glass

In his 1926 thesis Robert Cady Burts describes the production of sodium by electrolysis of sodium nitrate through glass. I can't find much else on this method. Are there any modern descriptions of ...
user17180's user avatar