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I want to create a thin film of elemental sulfur. Based on significant searching, I can find that elemental sulfur deposition is a significant problem in oil and gas. However, I cannot find any specifications for depositing elemental sulfur via CVD, ALD, or other methods.

Can anyone suggest a method for creating a thin film of elemental sulfur? Thanks!

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  • $\begingroup$ Evaporation would seem to be a direct way. The melting point is so low that it should be pretty easy in either a boat or e-gun system. Watch for sulfur-metal interactions on the boat. It may also react upon opening the system up. $\endgroup$ – Jon Custer Aug 7 '17 at 18:14
  • $\begingroup$ Can you explain a little more exactly what you mean? I have previously tried sublimation, as mentioned in the paper "A binder-free sulfur/carbon composite electrode prepared by a sulfur sublimation method for Li–S batteries" by Cui et al. However, I found that very little sulfur actually deposited and it was not possible to obtain a full film. However, my processing may have been imperfect. $\endgroup$ – User2341 Aug 7 '17 at 18:16
  • $\begingroup$ Reaction of copper sulfate and sodium thiosulfate in a 1 to 1 ratio. $\endgroup$ – AS_1000 Aug 20 '17 at 16:32

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