6
$\begingroup$

A Kipp's apparatus has three distinct bulbs. The topmost one contains a liquid and a tube to the bottommost one. The middle one contains a solid to react with the liquid.

Drawing of a filled Kipp's apparatus

This is very understandable when large chunks of solid are used. However, what do people do when they need to react a powder (e.g. sodium sulfite)? It seems that the powder would just fall through and keep reacting when the valve is closed.

$\endgroup$

2 Answers 2

3
$\begingroup$

According to the Wikipedia page on the Kipp's apparatus, if the reactant is a powder, and soluble in water, you can soak pieces of pumice in the solution, dry the pumice, and use it in a Kipp's apparatus. There is also a variant of the apparatus that allows two liquids to be used together rather than a liquid and a solid reactant. In that case, you would pre-dissolve the sodium sulfite in water.

$\endgroup$
3
$\begingroup$

There is an inner separator (a conical piece of glass emanating from the top of the base reservoir into which the stem from the top reservoir sits) which is perforated and acts to retain the solid in the middle chamber while allowing the acid to react (or not react) with the solid as the pressure in the system rises or falls.

See this detailed description with images for reference.

$\endgroup$

Your Answer

By clicking “Post Your Answer”, you agree to our terms of service and acknowledge that you have read and understand our privacy policy and code of conduct.

Not the answer you're looking for? Browse other questions tagged or ask your own question.