I think that answer would be:
Toluene and cyclohexane do not dissolve in water (since they are nonpolar), so I would first separate the water from the mixture with a separator funnel.
A mixture of cyclohexane and toluene would be separated by fractional distillation. Cyclohexane, which has a lower boiling point than toluene, would be eliminated from the mixture.
Is there anything wrong in my answer? Would there also be anything to add?